I’ve been sifting through some journals looking for the simplest protocol for the confirmation and concentration of an unknown sample, presumably stanozolol. I’m not quite a doctor of chemistry, several years from it, but I’ve got the ambition. I want to use as few reagents and/or instruments as possible. I’m not trying to identify conjugates (metabolites), just stanozolol. I was thinking of maybe LC/MS with methanol as the eluant would be a good and simple first approach.
Any knowledgable persons have any experience and/or suggestions with purification and/or identification?